| 第一部分 绪论(art one introduction) 一、物理化学实验的目的和要求 二、物理化学实验的安全知识 三、物理化学实验的设计思想 四、误差理论和有效数字 五、实验数据的表示法和处理 1．objective and requirement 2．hysical chemistry laboratory safety 3．rules for designing of the hysical chemistry exeriment 4．error theory and significant figures 5．data reorting第二部分 实验(art two exerjments) 实验一 燃烧热的测定 exeriment 1 heats of combustion 实验二 溶解热的测定 exenment 2 heats of solution 实验三 凝固点降低法测定摩尔质量和渗透压 exeriment 3 molar mass and osmotic：ressure by freezing ointderession 实验四 液体饱和蒸气压的测定 exenment 4 saturated vaor ressure of ure ljquids 实验五 反应平衡常数及分配系数的测定 exenment 5 equilibrium constant 0f reaction and aititimlcoefficient 实验六 完全互溶双液系平衡相图的绘制 exenment 6 hase diagram of a miscible binary liquid svstem 实验七 双组分简单低共熔体系相图的绘制 exenment 7 solid-liquid binary hase diagram 实验八 三组分液-液系统相图的绘制 exeriment 8 a ternary hase diagram for a system of threeliquids 实验九 电解质水溶液电导的测定及应用 exeriment 9 measurement and alication of electrolyte solution conductance 实验十 电动势法测溶液h和反应热力学函数 exeriment 10 determinations of h of solution and thermodynamicfunctions by electromotive force measurements 实验十一 一级反应速率常数的测定 exeriment 11 rate constant for first order reaction 实验十二 碘化钾与过氧化氢反应的速率常数及活化能的测定 exeriment 12 kinetics of reaction between otassium iodide andhydrogen eroxide 实验十三 丙酮溴化反应速率常数的测定 exeriment 13 rate constant and activation energy of thebromination of acetone 实验十四 乙酸乙酯皂化反应速率常数及活化能的测定 exeriment 14 rate constant for the saonification of ethylacetate by conductometric method 实验十五 最大泡压法测定溶液的表面张力 exeriment 15 surface tension of solutions by bubble ressuremethod 实验十六 固体在溶液中的吸附 exeriment 16 adsortion of solids in solution 实验十七 乳状液的制备和性质 exeriment 17 rearation and roerties of emulsion 实验十八 溶胶的制备及性质 exeriment 18 rearation and roerties of sols 实验十九 黏度法测定大分子的平均相对分子质量 exeriment 19 average relative molar mass of the macromolecule by viscosity method 实验二十 纳米材料的合成与表征(综合设计性试验) exeriment 20 rearation and characterization of nanomaterials (multi—designing exeriment) 实验二十一 药物稳定性及有效期测定(设计性实验) exeriment 21 determination of drug stability and shelf life (designing exeriment) 实验二十二 固体药物常规理化常数的测定(综合设计性实验)exeriment 22 hysical and chemical constants of drugs (multi—designing exeriment) 附录(aendices)常用物理化学数据表(reference data of exerimental hysical chemistry)参考文献(references) |
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