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Practical Organic Synthesis: A Student’s Guide实用有机合成： 学生指南

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Practical Organic Synthesis: A Student’s Guide实用有机合成： 学生指南

最 低 价：￥447.30

定 价：￥497.00

作 者：ReinhartKeese, Martin P. Brändle, Trevor P. Toube　著 著

出 版 社：

出版时间：2006-7-1

I S B N：9780470029664

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    内容简介
    　　Success in an experimental science such as chemistry depends on good laboratory practice, a knowledge of basic techniques, and the intelligent and careful handling of chemicals.
    　　Practical Organic Synthesis is a concise, useful guide to good laboratory practice in the organic chemistry lab with hints and tips on successful organic synthesis. Topics covered include:
    　　safety in the laboratory
    　　environmentally responsible handling of chemicals and solvents
    　　crystallisation
    　　distillation
    　　chromatographic methods
    　　extraction and work-up
    　　structure determination by spectroscopic methods
    　　searching the chemical literature
    　　laboratory notebooks
    　　writing a report
    　　hints on the synthesis of organic compounds
    　　disposal and destruction of dangerous materials
    　　drying and purifying solvents
    　　Practical Organic Synthesis is based on a successful course in basic organic chemistry laboratory practice which has run for several years at the ETH, Zurich and the University of Berne, and its course book Grundoperationen, now in its sixth edition.
    　　Condensing over 30 years of the authors’ organic laboratory teaching experience into one easy-to-read volume, Practical Organic Synthesis is an essential guide for those new to the organic chemistry laboratory, and a handy benchtop guide for practising organic chemists.

    作者简介

    目录
    preface
    CHAPTER 1 -Accident Prevention and First Aid
    　1.1 Safety
    　1.2 Avoiding Accidents
    CHAPTER 2-Environmentally Responsible Handling of Chemicals
    　and Solvents
    　2.1 Dangerous Materials: Poisons, Laws, Regulations and Classes
    　2.2 EU Poison Regulations
    　2.3 Concentration Limits
    　2.4 Chemical Carcinogens
    CHAPTER 3- Crystallisation
    CHAPTER 4- Distillation
    　4.1 Some Theoretical Considerations
    　4.2 Distillation in Practice
    CHAPTER 5-Chromatographic Methods
    　5.1 Basic Principles
    　5.2 Analytical and Preparative Thin-Layer Chromatography
    　5.3 Column Chromatography
    　5.4 Rapid Column Chromatography
    　5.5 HPLC
    CHAPTER 6-Extraction and Isolation
    　6.1 Separation of Mixtures According to Acidity
    CHAPTER 7- Structure Determination Using Spectroscopic Methods
    　7.1 Infrared Spectroscopy （IR）
    　7.2 Mass Spectrometry （MS）
    　7.3 Nuclear Magnetic Resonance Spectroscopy （NMR）
    　7.4 Ultraviolet and Visible Spectroscopy （UV/VIS）
    CHAPTER 8-Searching the Chemical Literature
    　8.1 The Information Mountain
    　8.2 Strategy
    　8.3 Databases
    　8.4 Reviews
    　8.5 Monographs, Reference Works and Handbooks
    　8.6 Data Collections
    CHAPTER 9-Laboratory Notebooks
    CHAPTER 1D-Writing a Report
    CHAPTER 11 -Example of a Laboratory Report
    CHAPTER 12-Hints on the Synthesis of Organic Compounds
    12.1 The Route to Success
    　12.2 Some Tips on Handling Water- and Air-Sensitive Substances
    　12.3 Hints on Working at Low Temperatures
    　12.4 Hints on the Synthesis and Analysis of Chiral Compounds
    　12.5 Hints on the Synthesis of Isotopically Labelled Compounds
    CHAPTER 13-Disposal and Destruction of Dangerous Materials
    　13.1 Classification of Waste Material
    　13.2 Environmentally Acceptable Substances for Treating Dangerous Materials in the Laboratory
    　13.3 Special Instructions for the Destruction of the Main Classes of Dangerous Substances
    　13.4 Deactivation of Unknown Laboratory Chemicals
    　13.5 Waste Disposal
    CHAPTER 14-Purification and Drying of Solvents
    　14.1 Some Drying Agents
    　14.2 Solvents
    CHAPTER 15-EU Rand SPhrases
    　15.1 R Phrases: Indication of Particular Risks
    　15.2 Combinations of R Numbers
    　15.3 S Phrases: Indication of Safety Precautions
    　15.4 Combinations of S Numbers

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